High-pressure low-temperature locknut cell for both EPR and NMR studies to 10 kilobars and 77 K

Sinha, Shantanu and Srinivasan, R (1983) High-pressure low-temperature locknut cell for both EPR and NMR studies to 10 kilobars and 77 K. In: Review of Scientific Instruments, 54 (11). pp. 1492-1496.

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Abstract

A locked high-pressure cell with working pressure range up to 10 kbars suitable for low-temperature studies to 77 K has been described. It can be used for both EPR and NMR studies of single crystals (and other solid samples). The high-pressure seal and all other aspects of the cell remain the same for either application. Only a change of the bottom plug is required for a switch from a nuclear-magnetic-resonance (NMR) to an electron-paramagnetic-resonance (EPR) experiment. Details of the procedure for the calibration of pressure inside the cell at various temperatures are discussed. The performance of the cell in EPR ($Cr^{3+}ion$) and NMR ($^{27}Al$ nucleus) studies is reported.

Item Type:	Journal Article
Publication:	Review of Scientific Instruments
Publisher:	American Institute of Physics
Additional Information:	Copyright of this article belongs to American Institute of Physics.
Department/Centre:	Division of Physical & Mathematical Sciences > Physics
Date Deposited:	14 Jul 2008
Last Modified:	19 Sep 2010 04:47
URI:	http://eprints.iisc.ac.in/id/eprint/15008

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