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Crystal growth of nanostructured zinc oxide nanorods from the seed layer

Adetoye, BO and Alabi, AB and Akomolafe, T and Managutti, PB and Coppede, N and Villani, M and Calestani, D and Zappetini, A and Maurizio, C (2018) Crystal growth of nanostructured zinc oxide nanorods from the seed layer. In: Materials Science- Poland, 36 (3). pp. 477-482.

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Official URL: https://doi.org/10.2478/msp-2018-0067

Abstract

One-dimensional (1D) zinc oxide (ZnO) nanostructures (nanorods) were synthesized on a glass slide and fluorine-doped tin oxide (SnO 2 /F or FTO) coated glass (FTO/glass) by a wet chemical method. The structural, morphological and optical analyses of the as-deposited ZnO nanostructures were performed by X-ray diffractometry (XRD), scanning electron microscopy (SEM) and UV-Vis spectroscopy, respectively. The XRD results showed that the nanostructures as-deposited on the glass and the FTO/glass substrates were of ZnO wurtzite crystal structure, and the crystallite sizes estimated from the (0 0 2) planes were 60.832 nm and 64.876 nm, respectively. The SEM images showed the growth of densely oriented ZnO nanorods with a hexagonal-faceted morphology. The UV-Vis absorption spectrum revealed high absorbance properties in the ultraviolet range and low absorbance properties in the visible range. The optical energy band gap of the ZnO nanostructure was estimated to be 3.87 eV by the absorption spectrum fitting (ASF) method.

Item Type: Journal Article
Publication: Materials Science- Poland
Publisher: Sciendo
Additional Information: The copyright for this article belongs to the Authors.
Keywords: Absorption spectra; Absorption spectroscopy; Crystal growth; Crystal structure; Energy gap; Glass; II-VI semiconductors; Nanocomposites; Nanostructures; Scanning electron microscopy; Tin oxides; Ultraviolet spectroscopy; Ultraviolet visible spectroscopy; X ray diffraction; X ray diffraction analysis; Zinc oxide; Zinc sulfide, Absorbance properties; Fluorine doped tin oxide; Nanostructured zinc oxides; Optical energy band gap; UV-VIS absorption spectra; UV-vis spectroscopy; Wet-chemical method; Wurtzite crystal structure, Nanorods
Department/Centre: Division of Chemical Sciences > Solid State & Structural Chemistry Unit
Date Deposited: 02 Sep 2022 03:56
Last Modified: 02 Sep 2022 03:56
URI: https://eprints.iisc.ac.in/id/eprint/76343

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