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Silicon tetrafluoride : Preparation and reduction with lithium aluminium hydride

Padma, DK and Suresh, BS and Vasudevamurthy, AR (1979) Silicon tetrafluoride : Preparation and reduction with lithium aluminium hydride. In: Journal of Fluorine Chemistry, 14 (4). pp. 327-329.

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Official URL: http://dx.doi.org/10.1016/S0022-1139(00)82975-9

Abstract

Pure silicon tetrafluoride can be prepared in 66% yield from silicon tetrachloride by refluxing with lead fluoride in acetonitrile. The gas can be reduced to pure silane by lithium aluminum hydride in diethyl ether.

Item Type: Journal Article
Publication: Journal of Fluorine Chemistry
Publisher: Elsevier Science
Additional Information: Copyright of this article belongs to Elsevier Science.
Department/Centre: Division of Chemical Sciences > Inorganic & Physical Chemistry
Date Deposited: 30 Nov 2010 11:02
Last Modified: 30 Nov 2010 11:02
URI: http://eprints.iisc.ac.in/id/eprint/34087

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