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Instant synthesis of nanoscale spinel aluminates

Mimani, T (2001) Instant synthesis of nanoscale spinel aluminates. In: Journal of Alloys and Compounds, 315 (1-2). pp. 123-128.

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Nanocryslalline metal aluminates MAl2O4, M=Mn, Cu and Zn have been prepared by the combustion of aqueous solutions containing corresponding metal acetate, aluminium nitrate, ammonium nitrate and different fuels, e.g., urea/carbohydrazide/oxalyldihydrazide I/hexamethylenetramine/glycine, The spinels obtained are nanosize (10-80 nm) oxides with surface area varying from 40 to 180 m(2)/g depending upon the fuel used. The products have been characterised by powder XRD and Al-27 MAS NMR spectroscopy. The particulate and morphological properties have been investigated using TEM and SEM techniques. Both ZnAl2O4 and CuAl2O4, prepared with carbohydlazide and glycine furls ale porous

Item Type: Journal Article
Publication: Journal of Alloys and Compounds
Publisher: Elsevier Science
Additional Information: Copyright of this article belongs to Elsevier Science.
Keywords: Nanostructures;Chemical synthesis;SEM/TEM/XRD;Phase transitions;Nuclear resonance.
Department/Centre: Division of Chemical Sciences > Inorganic & Physical Chemistry
Date Deposited: 25 Aug 2009 11:33
Last Modified: 19 Sep 2010 04:55
URI: http://eprints.iisc.ac.in/id/eprint/17052

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