Synthesis of size-controlled Bi particles by electrochemical deposition

Tharamani, CN and Thejaswini, HC and Sampath, S (2008) Synthesis of size-controlled Bi particles by electrochemical deposition. In: Bulletin of Materials Science, 31 (3). pp. 207-212.

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Abstract

Small sized bismuth particles are prepared by an electrochemical method using a triple voltage pulse technique. The bath composition and electrochemical parameters are optimized to yield monodisperse particles. The particles have been characterized by scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray analysis, X-ray photoelectron spectroscopy, UV-visible spectroscopy and X-ray diffraction technique. The particles, as deposited, are highly crystalline in nature and the particle size and shape get tuned depending on the conditions of deposition.

Item Type:	Journal Article
Publication:	Bulletin of Materials Science
Publisher:	Indian Academy of Sciences
Additional Information:	Copyright of this article belongs to Indian Academy of Sciences.
Keywords:	Bismuth nanoparticles;electrodeposition;SEM;TEM;XPS .
Department/Centre:	Division of Chemical Sciences > Inorganic & Physical Chemistry
Date Deposited:	06 Oct 2008 04:44
Last Modified:	19 Sep 2010 04:50
URI:	http://eprints.iisc.ac.in/id/eprint/16021

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