Chandran, Gopi R and Patil, KC (1990) A rapid combustion process for the preparation of crystalline mullite powders. In: Materials Letters, 10 (6). pp. 291-295.
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Abstract
An aqueous heterogeneous redox mixture containing aluminium nitrate, silica fume (soot), and urea in appropriate mole ratio, when rapidly heated to $500^{\circ}C$, boils, foams and ignites with a flame to yield weakly crystalline mullite powder in less than 5 min. Fully crystalline mullite was obtained by incorporating an extra amount of oxidizer, such as ammonium perchlorate. The solid combustion products (mullite) were identified by X-ray powder diffraction and characterized by IR, particle size analysis, surface area measurements, and by SEM and TEM microscopies.
Item Type: | Journal Article |
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Publication: | Materials Letters |
Publisher: | Elsevier Science B.V. |
Additional Information: | Copyright of this article belongs to Elsevier Science B.V. |
Department/Centre: | Division of Chemical Sciences > Inorganic & Physical Chemistry |
Date Deposited: | 19 Nov 2007 |
Last Modified: | 19 Sep 2010 04:41 |
URI: | http://eprints.iisc.ac.in/id/eprint/12524 |
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